Evaluation of Polydimethylsiloxane-Phenylsiloxane as a Coating for Stir Bar Sorptive Extraction

Yamile Pérez-Padilla, Saúl Ariel Medina Cetina, Alejandro Ávila-Ortega, Jesús Alberto Barrón-Zambrano, Alfredo Rafael Vilchis-Néstor, Cristian Carrera-Figueiras, David Muñoz Rodríguez

Abstract


Analytical pretreatment has become environmental-friendly because of material science assistance. In stir bar sorptive extraction (SBSE), a coating is typically used to isolate and preconcentrate organic compounds in aqueous samples. Here, a translucent coating based on polydimethylsiloxane and phenyltriethoxysilane was prepared by a sol-gel method. Characterization tests showed that the coating was homogeneous, relatively polar, and both thermally (< 400 °C) and chemically stable. Coated stir bars were evaluated in the SBSE experiments. Benzene derivatives were successfully extracted/preconcentrated from aqueous solutions and environmental waters. Furanic derivatives and antibiotics were moderately extracted from water, but they were extracted from isooctane.

Keywords


Sol-gel; polydimethylsiloxane; coating; SBSE; polyaromatics; furanics; antibiotics

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Płotka-Wasylka, J.; Szczepańska, N.; de la Guardia, M.; Namieśnik, J. TrAC Trends in Anal. Chem. 2015, 73, 19-38 DOI: https://doi.org/10.1016/j.trac.2015.04.026

Nogueira, J. M. F. TrAC Trends Anal. Chem. 2015, 71, 214–223 DOI: https://doi.org/10.1016/j.trac.2015.05.002

Rykowska, I.; Wasiak, W. Acta Chromatogr. 2013, 25, 27–46 DOI: https://doi.org/10.1556/AChrom.25.2013.1.13

Caruso, R.; Díaz-Parralejo, A.; Miranda, P.; Guiberteau, F. J. Mater. Res. 2001, 16, 2391–2398 DOI: https://doi.org/10.1557/JMR.2001.0328

Attia, S. M. J. Mater. Sci. Technol. 2002, 18, 211–218 DOI: 10.3321/j.issn:1005-0302.2002.03.005

Carbonell, D.; Barranco, V.; Jiménez-Morales, A.; Casal, B.; Galván, J. C. Colloid Polym. Sci. 2011, 289, 1875–1883 DOI: https://doi.org/10.1007/s00396-011-2504-y

Duraibabu, D.; Ganeshbabu, T.; Saravanan, P.; Kumar, S. A.; High Perform. Polym. 2014, 26, 725 – 733 DOI: https://doi.org/10.1177/0954008314528225

Kloskowski, A.; Pilarczyk, M.; Chrzanowski, W.; Namieśnik, J. Crit. Rev. Anal. Chem. 2010, 40, 172–186 DOI: https://doi.org/10.1080/10408347.2010.490486

Gilart, N.; Marcé, R. M.; Borrull, F.; Fontanals, N. TrAC Trends Anal. Chem. 2014, 54, 11–23 DOI: https://doi.org/10.1016/j.trac.2013.10.010

Li, J.; Li, F.; Liu, Q. Chemosphere 2017, 178, 143–153 DOI: https://doi.org/10.1016/j.chemosphere.2017.03.052

Nie, S. P.; Huang, J. G.; Zhang, Y. N.; Hu, J. L.; Wang, S.; Shen, M. Y.; Li, C.; Marcone, M. F.; Xie, M.Y. Food Control, 2013, 30, 62–68 DOI: https://doi.org/10.1016/j.foodcont.2012.07.020

Baran, W.; Adamek, E.; Ziemiańska, J.; Sobczak, A. J. Hazard. Mater. 2011, 196, 1-15 DOI: https://doi.org/10.1016/j.jhazmat.2011.08.082

Liu, W.; Wang, H.; Guan, Y. J. Chromatogr. A 2004, 1045, 15–22 DOI: https://doi.org/10.1016/j.chroma.2004.06.036

Lan, L.; Hu, B.; Yu, C. J. Chromatogr. A 2010, 1217, 7003–7009 DOI: https://doi.org/10.1016/j.chroma.2010.09.006

Ibrahim, W. A. W.; Keyon, A. S. A.; Prastomo, N.; Matsuda, A. J. Sol-Gel Sci. Technol. 2011, 59, 128–134 DOI: https://doi.org/10.1007/s10971-011-2470-3

Yoldas, B. E. J. Non. Cryst. Solids 1984, 63, 145–154 DOI: https://doi.org/10.1016/0022-3093(84)90393-4

Wen, J.; Wilkes, G. L. Chem. Mater. 1996, 8, 1667–1681 DOI: 10.1021/cm9601143

Katagiri, K.; Hasegawa, K.; Matsuda, A.; Tatsumisago, M.; Minami, T. J. Am. Ceram. Soc. 1998, 81, 2501–2503 DOI: 10.1111/j.1151-2916.1998.tb02653.x

Ma, M.; Zhang, Y.; Yu, W.; Shen, H.; Zhang, H.; Gu, N. Colloids Surfaces A Physicochem. Eng. Asp. 2003, 212, 219–226 DOI: https://doi.org/10.1016/S0927-7757(02)00305-9

Bange, J. P.; Patil, L. S.; Gautam, D. K. Prog. Electromagn. Res. M 2008, 3, 165–175 DOI: 10.2528/PIERM08060401

Rao, A. V.; Kalesh, R. R.; Pajonk, G. M. J. Mater. Sci. 2003, 38, 4407–4413 DOI: https://doi.org/10.1023/A:1026311905523

Park, J. T.; Seo, J. A.; Ahn, S. H.; Kim, J. H.; Kang, S. W. J. Ind. Eng. Chem. 2010, 16, 517–522 DOI: https://doi.org/10.1016/j.jiec.2010.03.030

Liu, L.; Sheardown, H. Biomaterials 2005, 26, 233–244 DOI: https://doi.org/10.1016/j.biomaterials.2004.02.025

Jopp, J.; Grüll, H.; Yerushalmi-Rozen, R. Langmuir 2004, 20, 10015–10019 DOI: 10.1021/la0497651

Yan, X.; Wu, D.; Peng, H.; Ding, K.; Duan, C.; Guan, Y. J Chromatogr A 2012, 69-76 DOI: https://doi.org/10.1016/j.chroma.2012.05.015

Bosworth, T.; Setford, S.; Saini, S.; Heywood, R. Anal. Chim. Acta. 2001, 450, 253–261 DOI: https://doi.org/10.1016/S0003-2670(01)01377-0




DOI: http://dx.doi.org/10.29356/jmcs.v62i2.431

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Copyright (c) 2018 Yamile Pérez-Padilla, Saúl Ariel Medina Cetina, Alejandro Ávila-Ortega, Jesús Alberto Barrón-Zambrano, Alfredo Rafael Vilchis-Néstor, Cristian Carrera-Figueiras, David Muñoz Rodríguez

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Journal of the Mexican Chemical Society (J. Mex. Chem. Soc.) Vol 62, No 2 (2018). Quarterly publication (April-June). Edited and distributed by Sociedad Química de México, A.C. Barranca del Muerto 26, Col. Crédito Constructor, Del. Benito Juárez, C.P. 03940, Mexico City. Phone: +5255 56626837; +5255 56626823 Contact: soquimex@sqm.org.mx http://www.sqm.org.mx Editor-in-Chief: Ignacio González-Martínez. Indexed Journal. Certificate of reserved rights granted by the Instituto Nacional del Derecho de Autor (INDAUTOR): 04-2005-052710530600-102. Certificate of lawful title and content: Under procedure. ISSN-e granted by the Instituto Nacional del Derecho de Autor (INDAUTOR): 2594-0317. ISSN granted by the Instituto Nacional del Derecho de Autor (INDAUTOR): 1870-249X. Postal registration of printed matter deposited by editors or agents granted by SEPOMEX: IM09-0312 Copyright © Sociedad Química de México, A.C. Total or partial reproduction is prohibited without written permission of the right holder. The Figures/schemes quality and the general contents of this publication are full responsibility of the authors. Updated June 6th, 2018 by Adriana Vázquez (editorial assistant, e-mail: editor.jmcs@gmail.com), J. Mex. Chem. Soc., Sociedad Química de México, A.C.